Название |
Intensification of pulp separation in beryllium production |
Информация об авторе |
All-Russian Research Institute of Chemical Technology, Moscow, Russia: V. A. Tolkachev, Leading Researcher N. P. Paskhin, Senior Researcher D. V. Maynikov, Senior Researcher, e-mail: didima06@mail.ru |
Реферат |
Ulba Metallurgical Plant applies the labor-intensive beryllium concentrate processing. In order to exclude this process from the production, we offer the concentrate opening in autoclave using sodium alkali in beryllium production technology. However, the pulps, formed after the alkali leaching, are hardly separated without flocculant additives and have low filtering rates. This is explained by a high degree of crushing of initial solid material and high alkali concentration used during leaching. Research results offered the methods of increasing the efficiency of pulp filtering and washing the sediments, obtained after alkaline opening of ore material. Production capacity of pulp filtering was considerably increased by CaO addition on the leaching stage. The pulp separation was significantly increased with simultaneous using CaO on the leaching stage and usage of flocculating agents for pulp thickening. Thickened flocculated pulps were filtered and washed under pressure with average production capacity of 30 kg/(m2·cycle). Having rather small consumption of rinsing water, the washing efficiency in all experiments was 99.9%. The filter-press with squeezed membranes is recommended for pulp filtering and sediments washing in industry. The obtained data may be used with further investigation of beryllium obtaining technology. This work was carried out within the Federal Target Program of the Ministry of Education and Science of the Russian Federation “Investigations and developments by the priority ways of development of the scientific and technological complex of Russia for 2014–2020”. Subsidiary agreement No. 14.582.21.0008, unique identifier of the agreement RFMEFI58215X0008. |
Библиографический список |
1. Matyasova V. E., Kotsar M. L., Kochubeeva S. L., Nikonov V. I. Generation of beryllium materials out of beryllium-containing wastes for nuclear and thermo-nuclear energetic. Voprosy atomnoy nauki i tekhniki. 2013. No. 2 (84). pp. 110–117. 2. Nesterov K. N., Radushinskiy S. M., Alekberov Z. M. Alkaline autoclave opening of beryllium concentrates on Ermakovskoe deposit. Tsvetnye Metally. 2017. No. 2. pp. 56–61. 3. Kislov E. V., Imetkhenov A. B., Sandakova D. M. The Yermakovskoye fluorite-beryllium deposit: avenues for improving ecological security of revitalization of the mining operations. Nauchnyy zhurnal geografiya i prirodnye resursy. 2010. No. 4. p. 30. 4. Matyasova V. E. Technology state and problems of organization of beryllium production in Russia. The 65 anniversary of VNIIKhT : collection of scientific proceedings. Moscow : LLC “Vinpress”, 2016. 5. Arinov B. Zh., Zorin B. L. Scientific-technological development of beryllium metallurgy on Ulba Metallurgical Plant. Tsvetnye Metally. 2011. No. 1. pp. 67–69. 6. Samoylov V. I. Improvement of the process of washing of sediment, forming in beryllium hydrometallurgy on raw material leaching stage. Tsvetnye Metally. 2007. No. 10. pp. 77–79. 7. Bearse А. Е., Calkins G. D., Clegg J. W., Filbert R. B. Thorium and rare earths from monazite. Chemical engineering progress. 1954. Vol. 50. pp. 235–239. 8. Gräfe M., Power G., Klauber C. Bauxite residue issues: III. Alkalinity and associated chemistry. Hydrometallurgy. 2011. No. 1–2, Vol. 108. pp. 60–79. 9. Yin-Fa Zhu, Jin-Yuan Qian, Qian-Kun Zhang, Ji-Yong Kuang, Xiao-Fei Gao, Zhi-Jiang Jin. Experimental analysis on filter press and energy consumption performance of diaphragm press drying device in chemical post-processing integrated equipment. Case Studies in Thermal Engineering. 2016. Vol. 7. pp. 92–102. 10. Zimin A. V., Kalinin E. P., Kutlin B. A. Khaibulla processing plant: Design solutions and construction. Eurasian mining. 2015. No. 1. pp. 49–52. 11. Beloglazov I. I., Bazhin V. Yu., Zyryanova O. V. Upgrading of the process of technological pulp separation in modern pressure filters. Non-ferrous Metals. 2016. No. 1. pp. 38–40. DOI: 10.17580/nfm.2016.01.07. 12. Zhen-guang Ru, Cen-xuan Pan, Gui-hua Liu, Xue-ting Wang, Guang-yu Dou, Ke-song Zhu. Leaching and recovery of zinc from leaching residue of zinc calcine based on membrane filter press. Transactions of Nonferrous Metals Society of China. 2015. Vol. 25, No. 2. pp. 622–627. 13. Jingzhen Zhang, Qinyan Yue, Chao Xia, Kunlun Yang, Pin Zhao, Baoyu Gao, Hui Yu. The study of Na2SiO3 as conditioner used to deep dewater the urban sewage dewatered sludge by filter press. Separation and Purification Technology. 2017. Vol. 174. pp. 331–337. |